抗生素检测


诺氟沙星(Norfloxacin),为第三代喹诺酮类抗菌药,会阻碍消化道内致病细菌的DNA旋转酶(DNA Gyrase)的作用,阻碍细菌DNA复制,对细菌有抑制作用,是治疗肠炎痢疾的常用药。


名称 CAS号 英文名称 简称 母离子m/z 子离子m/z(a为定量子离子) 内标物
诺氟沙星 70458-96-7 Norfloxacin NF 320.2 302.1a/276.2 环丙沙星-d8

标准曲线

抗生素检测

y = 0.41395 x + 1.15225 (r = 0.99824)


本底图谱


Sample Name Analyte Peak Name Area (cps) S/N Analyte RT(min) Target conc. () Calculated Concentration (ng/mL)
1 NF_1 1.815e4 14.3 3.52 N/A <0

本底图谱1

Sample Name Analyte Peak Name Area (cps) S/N Analyte RT(min) Target conc. () Calculated Concentration (ng/mL)
2 NF_1 1.346e4 13.4 3.82 N/A <0

本底图谱2

Sample Name Analyte Peak Name Area (cps) S/N Analyte RT(min) Target conc. () Calculated Concentration (ng/mL)
3 NF_1 2.277e4 10.4 3.54 N/A <0

本底图谱3

低标(加标100ng/L)图谱


Sample Name Analyte Peak Name Area (cps) S/N Analyte RT(min) Target conc. () Calculated Concentration (ng/mL)
4 NF_1 5.089e9 4491.6 3.82 N/A 128.09

低标(加标100ng/L)图谱1

Sample Name Analyte Peak Name Area (cps) S/N Analyte RT(min) Target conc. () Calculated Concentration (ng/mL)
5 NF_1 6.524e6 5717.7 3.82 N/A 127.27

低标(加标100ng/L)图谱2

Sample Name Analyte Peak Name Area (cps) S/N Analyte RT(min) Target conc. () Calculated Concentration (ng/mL)
6 NF_1 6.045e6 4925.8 3.83 N/A 119.31

低标(加标100ng/L)图谱2

高标(加标100ng/L)图谱


Sample Name Analyte Peak Name Area (cps) S/N Analyte RT(min) Target conc. () Calculated Concentration (ng/mL)
7 NF_1 1.121e7 7038.3 3.83 N/A 211.57
高标(加标100ng/L)图谱1

Sample Name Analyte Peak Name Area (cps) S/N Analyte RT(min) Target conc. () Calculated Concentration (ng/mL)
8 NF_1 1.366e7 6709.0 3.83 N/A 223.91

高标(加标100ng/L)图谱2

Sample Name Analyte Peak Name Area (cps) S/N Analyte RT(min) Target conc. () Calculated Concentration (ng/mL)
9 NF_1 1.398e7 2619.5 3.83 N/A 211.86
高(加标100ng/L)图谱3

低标加标回收率(范围 50%-200%):124.89%

高标加标回收率(范围 50%-200%):107.89%

低标精密度(3次重复标准偏差):3.88%

高标精密度(3次重复标准偏差):3.26%

Baidu
map